HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Nitro-2-phenylethane → (E)-6-nitro-7-phenylhept-5-enal
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Nitro-2-phenylethane | HCID 80208 | — |
| Edukt | Pentanal, 5,5-dimethoxy- | HCID 170903 | — |
| Lösungsmittel | Ethyl acetate hexane | HCID 21226206 | — |
| Produkt | (E)-6-nitro-7-phenylhept-5-enal | HCID 58434580 | 40% |
Reaktionsschritte
Prepared according to the general procedure B from 1-(2-nitroethyl)benzene 112e (24 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (1.49 g, 40% yield) after silica gel chromatography (EtOAc/Hexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08680335B2 |
| Quelldatensatz | uspto-grants-2014_03 |
| ORD ID | ord-7cf9d7b4aa8041be97c8ffed1f6d9b25 |
| Quellennotiz | uspto-grants-2014_03 |