HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Bromoethanol → (4R,9aR)-6-(2-Hydroxy-ethoxy)-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Bromoethanol | HCID 10898 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | (4R,9aR)-6-bromo-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester | HCID 86590113 | — |
| Edukt | HCID 178418747 | HCID 178418747 | — |
| Produkt | (4R,9aR)-6-(2-Hydroxy-ethoxy)-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester | HCID 69556691 | — |
Reaktionsschritte
This compound was prepared in analogy to Example 22 intermediate b), from (4R,9aR)-6-hydroxy-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester, sodium hydride and 2-bromoethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07098337B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-470b37aa1b554df0a01e828ed15e2e0e |
| Quellennotiz | uspto-grants-2006_08 |