Benzylamine → Benzeneacetamide, 4-hydroxy-N-(phenylmethyl)-

HRID 1193997Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1193997
CO[C:3](=[O:12])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1.[CH2:13]([NH2:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH2:13]([NH:20][C:3](=[O:12])[CH2:4][C:5]1[CH:6]=[CH:7][C:8]([OH:11])=[CH:9][CH:10]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Komponenten

3

Edukt 2

HCID 7504BenzylamineHCID 518900Benzeneacetic acid, 4-hydroxy-, methyl ester

Produkt 1

HCID 8376026Benzeneacetamide, 4-hydroxy-N-(phenylmethyl)-

Versuchsvorschrift

A mixture of 80 g of 4-hydroxyphenylacetic acid methyl ester and 51.6 g of benzylamine is brought to 180° C. for 8 hours. The mixture is allowed to return to room temperature and the crystals are filtered off and washed with ethanol and then ethyl ether.

Aufarbeitung

  1. customto return to room temperature
  2. filtrationthe crystals are filtered off
  3. washwashed with ethanol

Quellen und Nachweise

ORD-Eintrag
ord-e6cc62827f5340b38cecc8f52ef224c7
Quelldatensatz
uspto-grants-1989_03
Patentnummer
US04812469

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