HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfuric Acid → p-Tolylacetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | Lilac acetaldehyde | HCID 61006 | — |
| Edukt | Sodium Hypochlorite | HCID 23665760 | — |
| Produkt | p-Tolylacetic acid | HCID 248474 | — |
Reaktionsschritte
In the like manner as Example 1, 26.4 g of p-methylphenylacetaldehyde as an aldehyde and 2.3 g of sulfuric acid were used. The oxidation was done by using 125 g of 12% aqueous solution of sodium hypochlorite at temperatures of -10° to -12° C., which was followed by the hydrogenation to obtain p-methylphenylacetic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04814494 |
| Quelldatensatz | uspto-grants-1989_03 |
| ORD ID | ord-a6c0e22ac83543e18b5dba56bc8d265d |
| Quellennotiz | uspto-grants-1989_03 |