Thionyl Chloride → HCID 54224112, Verbindung
Reaktionsgleichung
[CH2:1]([C:10]1[CH:11]=[N:12][C:13]([C:16]2[CH:24]=[CH:23][C:19]([C:20](O)=[O:21])=[CH:18][CH:17]=2)=[N:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].S(Cl)([Cl:27])=O>>[CH2:1]([C:10]1[CH:11]=[N:12][C:13]([C:16]2[CH:24]=[CH:23][C:19]([C:20]([Cl:27])=[O:21])=[CH:18][CH:17]=2)=[N:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]Komponenten
3
Versuchsvorschrift
4-(5-n-Nonylpyrimidine-2-yl)benzoic acid (1.63 g) was heated together with excess thionyl chloride for 8 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 4-(5-n-nonylpyrimidine-2-yl)benzoic acid chloride.
Aufarbeitung
- temperatureunder reflux
- distillationunaltered thionyl chloride was distilled off
Quellen und Nachweise
- ORD-Eintrag
- ord-72305973013a49afb2087fbd4d249457
- Quelldatensatz