HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone → 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone | HCID 301557 | — |
| Edukt | Sodium hypobromite | HCID 23673712 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid | HCID 2759552 | 90% |
Reaktionsschritte
A solution of 18 g of 4-acetyl-4'-methoxybiphenyl in 285 ml of dioxane was oxidized with a dilute sodium hypobromite. Recrystallization from ethanol and acetic acid gave 4'-methoxybiphenyl-4-carboxylic acid melting at 285° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05114613 |
| Quelldatensatz | uspto-grants-1992_05 |
| ORD ID | ord-815353fc731c4aa0a12ab6f1fe7a78a7 |
| Quellennotiz | uspto-grants-1992_05 |