HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetaldehyde → HCID 14127108, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetaldehyde | HCID 177 | — |
| Edukt | Thiophene | HCID 8030 | — |
| Edukt | Benzamide, 4-(1-methylethyl)- | HCID 69277 | — |
| Lösungsmittel | Acetic acid sulfuric acid | HCID 23350293 | — |
| Produkt | HCID 14127108 | HCID 14127108 | 5% |
Reaktionsschritte
Thiophene (25 mmol), acetaldehyde (20 mmol) and 4-isopropylbenzamide (10 mmol) were stirred in a mixture of acetic acid/sulfuric acid (10 ml/0.2 ml) at 60° C. for one hour to obtain N-[1-(2-thienyl)ethyl]-4-isopropylbenzamide. Yield: 5%. A large part of the product was a tar-like material.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05117000 |
| Quelldatensatz | uspto-grants-1992_05 |
| ORD ID | ord-22e6f5daa7624279bcaab12778e7c1e6 |
| Quellennotiz | uspto-grants-1992_05 |