HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyldichlorosilane → Silane, dichloro-5-hexen-1-ylmethyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyldichlorosilane | HCID 6376 | — |
| Edukt | 1,5-Hexadiene | HCID 11598 | — |
| Edukt | 5-Hexenyldimethylchlorosilane | HCID 11829976 | — |
| Katalysator | Platinum | HCID 23939 | — |
| Produkt | Silane, dichloro-5-hexen-1-ylmethyl- | HCID 11063373 | 68% |
Reaktionsschritte
Procedure is similar to the one described above for 5-hexenyldimethylchlorosilane. 8.4 g (100 mmole) of 1,5-Hexadiene was refluxed with platinum catalyst (100ppm). To the mixture 5.7 g (50 mmole) of methyldichlorosilane was added dropwise over 30 min. period. The completion of the reaction was monitored by infrared spectroscopy. The product distilling at 65° C./0.22 mm was obtained in 68% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05278244 |
| Quelldatensatz | uspto-grants-1994_01 |
| ORD ID | ord-29bfa71d9dec400bb8337b4921eda113 |
| Quellennotiz | uspto-grants-1994_01 |