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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1197898Erstellt: 26. Oktober 2026

Methyldichlorosilane → Silane, dichloro-5-hexen-1-ylmethyl-

https://huagongshe.com/reaction/1197898

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyldichlorosilaneHCID 6376—
Edukt1,5-HexadieneHCID 11598—
Edukt5-HexenyldimethylchlorosilaneHCID 11829976—
KatalysatorPlatinumHCID 23939—
ProduktSilane, dichloro-5-hexen-1-ylmethyl-HCID 1106337368%

Reaktionsschritte

Procedure is similar to the one described above for 5-hexenyldimethylchlorosilane. 8.4 g (100 mmole) of 1,5-Hexadiene was refluxed with platinum catalyst (100ppm). To the mixture 5.7 g (50 mmole) of methyldichlorosilane was added dropwise over 30 min. period. The completion of the reaction was monitored by infrared spectroscopy. The product distilling at 65° C./0.22 mm was obtained in 68% yield.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05278244
Quelldatensatzuspto-grants-1994_01
ORD IDord-29bfa71d9dec400bb8337b4921eda113
Quellennotizuspto-grants-1994_01