HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Diacetylbenzene → alpha1,alpha3-Dimethyl-1,3-benzenedimethanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Diacetylbenzene | HCID 23229 | — |
| Edukt | Sodium borohydride | HCID 4311764 | — |
| Produkt | alpha1,alpha3-Dimethyl-1,3-benzenedimethanol | HCID 15148377 | — |
Reaktionsschritte
This mixture of stereoisomers was prepared from 1,3-diacetylbenzene by reduction with sodium borohydride as described above for the para stereoisomers. The mixture of stereoisomers was isolated as a semisolid. It appeared as a single spot on TLC and as a single peak on VPC.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05280096 |
| Quelldatensatz | uspto-grants-1994_01 |
| ORD ID | ord-828293c7f29e4075b17cc23d840ed7d7 |
| Quellennotiz | uspto-grants-1994_01 |