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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 11985Erstellt: 23. Oktober 2026

Propionitrile → HCID 178432489, Verbindung

https://huagongshe.com/de/reaction/11985

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPropionitrileHCID 7854—
Edukt1,2-DimethylbenzimidazoleHCID 312693—
EduktDisulfide, bis(2-bromoethyl)HCID 572268—
ProduktHCID 178432489HCID 178432489—

Reaktionsschritte

2.4 g of 1,2-dimethylbenzimidazole, 2.1 g of bis(2-bromoethyl) disulfide and 6 ml of propionitrile were stirred at 100 C in a sealed 20 ml reactor for 8 h. After cooling, filtration, washing with 3 times 10 ml and drying under vacuum, 2.2 g of beige solid were recovered. The analyses showed that the product was in conformity with the expected structure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07727287B2
Quelldatensatzuspto-grants-2010_06
ORD IDord-6ecb22d1266e4ad1878d98cb3b30a37b
Quellennotizuspto-grants-2010_06