HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-[3-(1,3-Dioxolan-2-yl)benzyl]-7-cyanomethoxyindole → 1-(3-Formylbenzyl)-7-cyanomethoxyindole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-[3-(1,3-Dioxolan-2-yl)benzyl]-7-cyanomethoxyindole | HCID 19102603 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 1-(3-Formylbenzyl)-7-cyanomethoxyindole | HCID 19102602 | — |
Reaktionsschritte
A solution of 1-[3-(1,3-dioxolan-2-yl)benzyl]-7-cyanomethoxyindole (50 mg., 0.15 mmol) in tetrahydrofuran (1 ml) and 2M hydrochloric acid (0.5 ml) was stirred at room temperature for 1 hour, diluted with water and extracted with ethyl acetate. The extract was dried and evaporated to a dark oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05281593 |
| Quelldatensatz | uspto-grants-1994_01 |
| ORD ID | ord-4eacd652e3ad4561be202fad9bfb3a9f |
| Quellennotiz | uspto-grants-1994_01 |