HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
m-Chloroperbenzoic acid → N-tert-Butyl-a-phenylnitrone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | m-Chloroperbenzoic acid | HCID 70297 | — |
| Edukt | N-(1,1-Dimethylethyl)benzenemethanamine | HCID 76908 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | N-tert-Butyl-a-phenylnitrone | HCID 4390 | — |
Reaktionsschritte
Following the general procedure of Example 1, N-benzyl-N-tert-butylamine is oxidized using a solution of 3-chloroperoxybenzoic acid dissolved in methylene chloride to give N-tert-butyl-alpha-phenyl nitrone as a white solid melting at 70°-72° C. This is the nitrone described in Japanese Sho No. 59-11345.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04898901 |
| Quelldatensatz | uspto-grants-1990_02 |
| ORD ID | ord-4cea29d3563046168c242b9deb9efc7b |
| Quellennotiz | uspto-grants-1990_02 |