HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(+-)-Pantolactone → Keto-pantoyllactone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (+-)-Pantolactone | HCID 989 | — |
| Katalysator | Molybdenum trioxide | HCID 14802 | — |
| Katalysator | Hematite (Fe2O3) | HCID 14833 | — |
| Produkt | Keto-pantoyllactone | HCID 39 | — |
Reaktionsschritte
A mixture of iron (III) oxide and molybdenum trioxide (G-105 from Girdler) is used as the catalyst in the reactor described in Example 1 and the temperature of the air bath is adjusted to 225° C. 60 l of air and 33 g of pantolactone are subsequently added hourly to the evaporator. 96% of the pantolactone are transformed and ketopantolactone is formed with a selectivity of 83%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04904805 |
| Quelldatensatz | uspto-grants-1990_02 |
| ORD ID | ord-c781faa2b1a44c349a9a32b4dad84e85 |
| Quellennotiz | uspto-grants-1990_02 |