HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Iodophenol → 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Iodophenol | HCID 10784 | — |
| Edukt | Phenylboronic acid pinacol ester | HCID 570673 | — |
| Produkt | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734623 | — |
Reaktionsschritte
The above reaction procedure used for 2-iodophenol was followed. The reaction was faster, being complete before the first sample for gc analysis was withdrawn after 1 h 50 min reaction time. The amount of phenylboronic acid pinacol ester was higher than in the 2-iodophenol reaction (around 7%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07122694B2 |
| Quelldatensatz | uspto-grants-2006_10 |
| ORD ID | ord-23004de992854d06895bd83361499298 |
| Quellennotiz | uspto-grants-2006_10 |