HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Ethoxy-1-(3-pyridinyl)-2-propen-1-one → Phenyl[7-(3-pyridinyl)pyrazolo[1,5-a]pyrimidin-3-yl]methanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Ethoxy-1-(3-pyridinyl)-2-propen-1-one | HCID 54032326 | — |
| Edukt | HCID 178509267 | HCID 178509267 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | Phenyl[7-(3-pyridinyl)pyrazolo[1,5-a]pyrimidin-3-yl]methanone | HCID 13475883 | — |
Reaktionsschritte
A mixture of 0.02 mole of 3-ethoxy-1-(3-pyridinyl)-2-propen-1-one, 0.02 mole of (3-amino-1H-pyrazol-4-yl)phenyl-methanone and 100 ml of xylene was refluxed for 12 hours. The solvent was removed and the residue dissolved in dichloromethane. This solution was dried over sodium sulfate and the product isolated as described in Example 1, as crystals, mp 202°-203° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04521422 |
| Quelldatensatz | uspto-grants-1985_06 |
| ORD ID | ord-c49638eb094243959a97d943725eda29 |
| Quellennotiz | uspto-grants-1985_06 |