Dimethylamine → HCID 12797674, Verbindung

HRID 1249113

Reaktionsgleichung

Reaktionsgleichung von HRID 1249113
[CH3:1][NH:2][CH3:3].[Cl:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[N:11]=[C:10]([O:15][C:16]1[CH:27]=[CH:26][C:19]([O:20][CH:21]([CH3:25])[C:22]([OH:24])=[O:23])=[CH:18][CH:17]=1)[CH:9]=[N:8]2>>[Cl:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[N:11]=[C:10]([O:15][C:16]1[CH:17]=[CH:18][C:19]([O:20][CH:21]([CH3:25])[C:22]([OH:24])=[O:23])=[CH:26][CH:27]=1)[CH:9]=[N:8]2.[CH3:1][NH:2][CH3:3]

Komponenten

3

Edukt 2

HCID 674DimethylamineHCID 178795Quizalofop

Produkt 1

HCID 12797674HCID 12797674, VerbindungAusbeute 91 %

Versuchsvorschrift

In 30 ml. of 10% aqueous solution of dimethylamine, 3.4 g. (0.01 mole) of 2-[4-(6-chloro-2-quinoxalyloxy)phenoxy]propionic acid was added. After a dissolution, excess of dimethylamine and water were removed by evaporating them by a rotary evaporator and the residue was dried in vacuum to obtain 3.5 g. (yield: 91%) of a pale yellow object product having a melting point of 63° to 67° C.

Aufarbeitung

  1. dissolutionAfter a dissolution
  2. customexcess of dimethylamine and water were removed
  3. customby evaporating them
  4. customby a rotary evaporator
  5. customthe residue was dried in vacuum
  6. customto obtain 3.5 g

Quellen und Nachweise

ORD-Eintrag
ord-a32bfccf63e94fdaaa45716d226bb358
Quelldatensatz
uspto-grants-1986_12
Patentnummer
US04629493

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