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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1249284Erstellt: 26. Oktober 2026

Hydrochloric Acid → HCID 73348316, Verbindung

https://huagongshe.com/reaction/1249284

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
EduktWaterHCID 962—
Edukt61036-62-2HCID 16131923—
Lösungsmittel1,1,2-TrichloroethanolHCID 119427—
ProduktHCID 73348316HCID 73348316—

Reaktionsschritte

2.5 g of teicoplanin complex (i.e. the antibiotic complex containing teichomycin factors A1, A2 and A3, as obtained by fermentation of strain ATCC 31121 according to U.S. Pat. No. 4,239,751, the water content determined by Karl-Fischer method is 13.5% by weight) is suspended in 50 ml of trichloroethanol and the mixture is stirred at 90° C. for 12 hours while continuously bubbling anhydrous hydrogen chloride. The reaction mixture is then worked up as in Example 11 yielding 700 mg of substantially pure deglucoteicoplanin.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04629781
Quelldatensatzuspto-grants-1986_12
ORD IDord-5e821c6044a948e18566f87a9ce74a01
Quellennotizuspto-grants-1986_12