HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Allylamine → 2-Allylamino-4-dodecylamino-6-nitroquinazoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Allylamine | HCID 7853 | — |
| Edukt | 2-Chloro-4-dodecylamino-6-nitroquinazoline | HCID 18326516 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-Allylamino-4-dodecylamino-6-nitroquinazoline | HCID 18326548 | 93,4% |
Reaktionsschritte
To 170 mg (0.44 mmol) of 2-chloro-4-dodecylamino-6-nitroquinazoline was added 1.70 ml (22.66 mmol) of allylamine, and then the resulting mixture was stirred at room temperature overnight. After water was added to the reaction solution, crystals thus precipitated were filtered to give 170 mg (93.4%) of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06339089B2 |
| Quelldatensatz | uspto-grants-2002_01 |
| ORD ID | ord-46e3260cc7e241ce9c3303d32471a74b |
| Quellennotiz | uspto-grants-2002_01 |