HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-{3-[(3-Morpholinopropyl)amino]-3-oxopropyl}phenyl N-octadecylcarbamate → HCID 18520278, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-{3-[(3-Morpholinopropyl)amino]-3-oxopropyl}phenyl N-octadecylcarbamate | HCID 9809286 | — |
| Edukt | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | HCID 18520278 | HCID 18520278 | — |
Reaktionsschritte
4N Hydrochloric acid/ethyl acetate solution (0.10 ml) was added to a solution containing 2-{3-[(3-morpholinopropyl)amino]-3-oxopropyl}phenyl N-octadecylcarbamate (0.20 g) in ethyl acetate (2 ml) while being cooled with ice. After being stirred for 30 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (0.19 g) as white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06339154B1 |
| Quelldatensatz | uspto-grants-2002_01 |
| ORD ID | ord-3eaea26ef3564063b69408a7b1fae71c |
| Quellennotiz | uspto-grants-2002_01 |