HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Vinylpyrrolidine → Ethyl 5-(4-ethylphenyl)-6-phenylpyridine-2-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Vinylpyrrolidine | HCID 3014294 | — |
| Edukt | Ethyl 6-(4-ethyl-phenyl)-5-phenyl-1,2,4-triazine-3-carboxylate | HCID 25033000 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | Ethyl 5-(4-ethylphenyl)-6-phenylpyridine-2-carboxylate | HCID 25033078 | — |
Reaktionsschritte
Following General Procedure D, ethyl 6-(4-ethyl-phenyl)-5-phenyl-1,2,4-triazine-3-carboxylate (Compound 13, 105 mg, 0.30 mmol) and crude 1-vinylpyrrolidine (Compound 38, 2 g) in CHCl3 (10 ml) were reacted to produce the title compound as a yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07728014B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-ff9619e76cab447082841ad9a3fd4058 |
| Quellennotiz | uspto-grants-2010_06 |