Benzyl Bromide → HCID 14155410, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[C:9]([Cl:10])=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][OH:5].[CH2:11](Br)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:5][CH2:4][C:3]1[CH:6]=[CH:7][CH:8]=[C:9]([Cl:10])[C:2]=1[NH2:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1Komponenten
3
Versuchsvorschrift
This material was prepared from 2-amino-3-chlorobenzyl alcohol and benzyl bromide by the general procedure outlined in Example 82. The product was purified by Kugelrohr distillation to yield an oil, bp 118°-125° C. (0.1 mm). The product was characterized by IR and 1H NMR spectroscopy.
Aufarbeitung
- distillationThe product was purified by Kugelrohr distillation
- customto yield an oil, bp 118°-125° C. (0.1 mm)
Quellen und Nachweise
- ORD-Eintrag
- ord-033dc7c8b3b9456183f05a93ad1d0f19
- Quelldatensatz
- uspto-grants-1988_05
- Patentnummer
- US04741764
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