Diethanolamine → N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-diethanolamine

HRID 1252035Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1252035
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[NH:23]([CH2:27][CH2:28][OH:29])[CH2:24][CH2:25][OH:26]>>[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([N:23]([CH2:27][CH2:28][OH:29])[CH2:24][CH2:25][OH:26])=[O:6]

Komponenten

3

Edukt 2

HCID 8113DiethanolamineHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

Produkt 1

HCID 54303147N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-diethanolamineAusbeute 90 %

Versuchsvorschrift

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 2.9 ml of diethanolamine were used as starting materials. 7.0 g (yield 90%) of the title compound was obtained as a colorless oil. Elemental analysis for C24H41NO3

Quellen und Nachweise

ORD-Eintrag
ord-5d4dd734f203420381a2f8082db06189
Quelldatensatz
uspto-grants-1988_05
Patentnummer
US04742058

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