HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Vinylpyrrolidine → Ethyl 5-phenyl-6-(4-trifluoromethylphenyl)-pyridine-2-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Vinylpyrrolidine | HCID 3014294 | — |
| Edukt | Ethyl 5-(4-trifluoromethylphenyl)-6-phenyl-1,2,4-triazine-3-carboxylate | HCID 59338807 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | Ethyl 5-phenyl-6-(4-trifluoromethylphenyl)-pyridine-2-carboxylate | HCID 68407826 | — |
Reaktionsschritte
Following General Procedure D, ethyl 5-(4-trifluoromethylphenyl)-6-phenyl-1,2,4-triazine-3-carboxylate (Compound 19, 1 g, 2.68 mmol) and crude 1-vinylpyrrolidine (Compound 38, 1.4 g) in CHCl3 (20 ml) were reacted to produce the title compound as a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07728014B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-44b6bfd75d794d3281b750bfa16d6f38 |
| Quellennotiz | uspto-grants-2010_06 |