2-(Trifluoromethyl)acrylic acid → 3-Acetylthio-2-trifluoromethylpropanoic acid

HRID 1252806

Reaktionsgleichung

Reaktionsgleichung von HRID 1252806
[C:1]([OH:6])(=[S:5])[CH:2](C)O.[F:7][C:8]([F:15])([F:14])[C:9](=[CH2:13])[C:10]([OH:12])=[O:11]>>[C:1]([S:5][CH2:13][CH:9]([C:8]([F:15])([F:14])[F:7])[C:10]([OH:12])=[O:11])(=[O:6])[CH3:2]

Komponenten

3

Edukt 2

HCID 5876942-(Trifluoromethyl)acrylic acidHCID 178473673HCID 178473673, Verbindung

Produkt 1

HCID 128330143-Acetylthio-2-trifluoromethylpropanoic acid

Versuchsvorschrift

A mixture of thiolactic acid (50 g) and 2-(trifluoromethyl)acrylic acid [M. W. Buxton, et al., J. Chem Soc., 366 (1954)] (66 g) is heated on the steam bath for one hour and then stored at room temperature for eighteen hours. The reaction mixture is distilled in vacuo to give 3-acetylthio-2-trifluoromethylpropanoic acid.

Aufarbeitung

  1. temperatureis heated on the steam bath for one hour
  2. waitstored at room temperature for eighteen hours
  3. distillationThe reaction mixture is distilled in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-460d5ee2dd4142559165013c581f2b6b
Quelldatensatz
uspto-grants-1988_05
Patentnummer
US04745124

Verknüpfte Notizen

Wird geladen…