HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonium Chloride → 5-(4-[2-Propylguanidino]pyrimid-2-yl)valeramidine hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonium Chloride | HCID 25517 | — |
| Edukt | Methyl 5-(4-[2-propylguanidino]pyrimid-2-yl)valerimidate | HCID 20137162 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 5-(4-[2-Propylguanidino]pyrimid-2-yl)valeramidine hydrochloride | HCID 20137149 | 93,2% |
Reaktionsschritte
A mixture of methyl 5-(4-[2-propylguanidino]pyrimid-2-yl)valerimidate (0.4 g.) and ammonium chloride (0.076 g.) in MeOH (20 ml.) was stirred at ambient temperature for 1 hour and the solvent evaporated in vacuo to give 5-(4-[2-propylguanidino]pyrimid-2-yl)valeramidine hydrochloride (0.4 g.) as an oil which was used without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04748165 |
| Quelldatensatz | uspto-grants-1988_05 |
| ORD ID | ord-9f68561694d34a0d9c0e9e77265079fc |
| Quellennotiz | uspto-grants-1988_05 |