2-Methyl-4-[(4-methylbenzenesulfonyl)oxy]butan-2-ol → 4-(5-Bromo-4,6-dimethylpyridin-2-yloxy)-2-methylbutan-2-ol
Reaktionsgleichung
[Br:1][C:2]1[C:3]([CH3:10])=[CH:4][C:5]([OH:9])=[N:6][C:7]=1[CH3:8].CC1C=CC(S(O[CH2:22][CH2:23][C:24]([OH:27])([CH3:26])[CH3:25])(=O)=O)=CC=1>>[Br:1][C:2]1[C:3]([CH3:10])=[CH:4][C:5]([O:9][CH2:22][CH2:23][C:24]([CH3:26])([OH:27])[CH3:25])=[N:6][C:7]=1[CH3:8]Komponenten
3
Versuchsvorschrift
According to a method described in [WO 2009/054423 pamphlet, (Production Example 37)], from 5-bromo-4,6-dimethyl-2-hydroxypyridine (1.50 g) and 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate (2.11 g), the subject compound (1.50 g) was obtained as a colorless oil.
Quellen und Nachweise
- ORD-Eintrag
- ord-743b476f845d4cebb8691bd3a5e7e018
- Quelldatensatz
- uspto-grants-2013_06
- Patentnummer
- US08455500B2
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