HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 3-[(Pyrrolidin-1-yl)methyl]benzoic acid hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Methyl 3-(pyrrolidin-1-ylmethyl)benzoate | HCID 53429637 | — |
| Produkt | 3-[(Pyrrolidin-1-yl)methyl]benzoic acid hydrochloride | HCID 18525874 | — |
Reaktionsschritte
A solution of 3-pyrrolidin-1-ylmethyl-benzoic acid methyl ester (800 mg, 3.6 mmol) in aqueous 25% hydrochloric acid (15 mL) was stirred at 90° C. for 4 hours. The solvent was evaporated affording the title compound as brown oil (quantitative) that was used as such for the next step.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08461193B2 |
| Quelldatensatz | uspto-grants-2013_06 |
| ORD ID | ord-13aa797902c049a9a0a2029f555dbccb |
| Quellennotiz | uspto-grants-2013_06 |