HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dilauryl Ether → 2-Methylundecane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dilauryl Ether | HCID 20667 | — |
| Edukt | Trifluoromethanesulfonic acid | HCID 62406 | — |
| Edukt | 10-Methyl-1-undecene | HCID 519941 | — |
| Edukt | Isododecanol | HCID 6428591 | — |
| Produkt | 2-Methylundecane | HCID 23459 | — |
Reaktionsschritte
300.0 g Lial® 123 (isododecanol from Sasol) and 18.0 g trifluoromethanesulfonic acid (50% by weight in water) were introduced into a distillation apparatus and heated for 1.5 h to 240° C. The organic phase of the distillate obtained (171.9 g) was dried over sodium sulfate and the product was isolated by filtration). The product then contained 91.5% isododecene, 7.5% Lial® 123 and 1.0% didodecyl ether (GC analysis).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08461407B2 |
| Quelldatensatz | uspto-grants-2013_06 |
| ORD ID | ord-48894196fe9f4034a9a0c2e7526108e1 |
| Quellennotiz | uspto-grants-2013_06 |