HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → 4-Chloro-N-methyl-2-nitro-5-(4-trifluoromethyl-piperidin-1-yl)aniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 4-(Trifluoromethyl)piperidine | HCID 136469 | — |
| Edukt | 4,5-Dichloro-n-methyl-2-nitroaniline | HCID 289317 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | 4-Chloro-N-methyl-2-nitro-5-(4-trifluoromethyl-piperidin-1-yl)aniline | HCID 44120655 | — |
Reaktionsschritte
The sub-title compound was prepared from 4,5-dichloro-2-nitro-N-methyl-aniline (820 mg, 3.7 mmol), 4-trifluoromethyl-piperidine (680 mg, 4.5 mmol) and potassium carbonate (770 mg, 5.6 mmol) in DMSO (10 mL) in analogy to example 3, step (a).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08466186B2 |
| Quelldatensatz | uspto-grants-2013_06 |
| ORD ID | ord-9240ae367e324c91b9e6d9ef1785bbb1 |
| Quellennotiz | uspto-grants-2013_06 |