Triethylamine → 2,4,6-Triiodophenyl penta-4-enoate
Reaktionsgleichung
[CH:1]1[C:2]([I:10])=[CH:3][C:4]([I:9])=[C:5]([OH:8])[C:6]=1[I:7].[C:11](Cl)(=[O:16])[CH:12]=[CH:13][CH2:14][CH3:15].C(N(CC)CC)C>ClCCl>[C:11]([O:8][C:5]1[C:6]([I:7])=[CH:1][C:2]([I:10])=[CH:3][C:4]=1[I:9])(=[O:16])[CH2:12][CH2:13][CH:14]=[CH2:15]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
First, 9 g of triiodophenol was dissolved in 150 mL dichloromethane under argon. Then, 3.15 mL of pentenoyl chloride was added while stirring. Triethylamine was then added slowly and stirred for 4 hr. The solution was washed with 100 mL of water and evaporated to dryness, leaving 2,4,6-triiodophenyl penta-4-enoate.
Aufarbeitung
- stirringstirred for 4 hr
- washThe solution was washed with 100 mL of water
- customevaporated to dryness
Quellen und Nachweise
- ORD-Eintrag
- ord-f5ec7c7b42c14d5aadebb227c5c52ac9
- Quelldatensatz
- uspto-grants-2013_06
- Patentnummer
- US08470035B2
Notizen zur Reaktion
Wird geladen…