2,6-Dimethylphenol → HCID 28971738, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[CH3:16]C1C=CC=C(C)C=1O>>[CH3:1][C:2]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:3]=1[O:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]Komponenten
3
Versuchsvorschrift
5-(2,6-Dimethylphenoxy)pentanoic acid 26c was prepared in the same manner as 26b, except that 2,6-dimethylphenol was used as the starting material. 1H NMR: (400 MHz, CDCl3): 7.0-7.1 (m, 3H), 3.83 (t, 2H, J=6 Hz), 2.37 (t, 2H, J=6 Hz), 2.73 (s. 6H), 1.92 (m, 4H). MS (ESI): 223 [M+H]+; 245 [M+Na]+.
Quellen und Nachweise
- ORD-Eintrag
- ord-4610f6f4060e4bcb8d2a00561c11ccae
- Quelldatensatz
- uspto-grants-2013_06
- Patentnummer
- US08470861B2
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