HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formic Acid → Methyl 4-formamidothiophene-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formic Acid | HCID 284 | — |
| Edukt | Methyl 4-aminothiophene-3-carboxylate | HCID 2777610 | — |
| Edukt | Sodium Acetate Trihydrate | HCID 23665404 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Methyl 4-formamidothiophene-3-carboxylate | HCID 2777637 | — |
Reaktionsschritte
A stirred solution of methyl 4-amino-3-thenoate (4 g), sodium acetate trihydrate (2.8 g) and formic acid (27 ml) was heated at 95° C. for 1 hour. On cooling the solution was poured into water, and the solution filtered to give the title product as a solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06541630B1 |
| Quelldatensatz | uspto-grants-2003_04 |
| ORD ID | ord-1f8a736f815c4486ba73f995478a54f7 |
| Quellennotiz | uspto-grants-2003_04 |