2-Fluorophenylboronic acid → HCID 69688386, Verbindung
Reaktionsgleichung
[C:1]([O:5][C:6](=[O:24])[NH:7][C:8]1[CH:13]=[C:12]([O:14][CH2:15][C:16]([F:19])([F:18])[F:17])[C:11](I)=[CH:10][C:9]=1[N+:21]([O-:23])=[O:22])([CH3:4])([CH3:3])[CH3:2].[F:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1B(O)O>>[C:1]([O:5][C:6](=[O:24])[NH:7][C:8]1[C:9]([N+:21]([O-:23])=[O:22])=[CH:10][C:11]([C:27]2[CH:28]=[CH:29][CH:30]=[CH:31][C:26]=2[F:25])=[C:12]([O:14][CH2:15][C:16]([F:19])([F:18])[F:17])[CH:13]=1)([CH3:4])([CH3:3])[CH3:2]Komponenten
3
Versuchsvorschrift
The title compound was prepared from [4-iodo-2-nitro-5-(2,2,2-trifluoro-ethoxy)-phenyl]-carbamic acid tert.-butyl ester (Example B4) and 2-fluorophenylboronic acid according to the general procedure D. Obtained as a yellow solid (1.39 g).
Quellen und Nachweise
- ORD-Eintrag
- ord-49c745b486cc4e77903e00272d4780ad
- Quelldatensatz
- uspto-grants-2003_04