HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548717 | — |
Reaktionsschritte
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (5.94 g, 25 mmol), methanol (25 mL) and KOH (1.98 g, 30 mmol) in DMSO (25 mL) according to the general procedure E. Obtained as an orange solid (5.88 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06548495B2 |
| Quelldatensatz | uspto-grants-2003_04 |
| ORD ID | ord-e6ee15db5ebc44d9980b62679a2b0bb5 |
| Quellennotiz | uspto-grants-2003_04 |