Benzene, 1-chloro-4-(1,1-dimethylethyl)- → HCID 23435198, Verbindung
Reaktionsgleichung
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([C:13]2[CH:18]=[CH:17][C:16]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:15][CH:14]=2)=O)=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[C:23]([C:27]1[CH:32]=[CH:31][C:30]([Cl:33])=[CH:29][CH:28]=1)([CH3:26])([CH3:25])[CH3:24]>>[Cl-:33].[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S+:11]([C:30]2[CH:31]=[CH:32][C:27]([C:23]([CH3:26])([CH3:25])[CH3:24])=[CH:28][CH:29]=2)[C:13]2[CH:18]=[CH:17][C:16]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:15][CH:14]=2)=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2]Komponenten
3
Versuchsvorschrift
The end compound was synthesized as in Synthesis Example 2 except that bis(4-tert-butylphenyl) sulfoxide was used instead of the phenyl sulfoxide in Synthesis Example 2, 4-tert-butylchlorobenzene was used instead of the chlorobenzene, and the quantity of water for extraction was increased.
Aufarbeitung
- extractionthe quantity of water for extraction
- temperaturewas increased