1,1,1,2,2-Pentafluoro-5-iodopentane → Ethyl 2-(4,4,5,5,5-pentafluoropentyl)-9-decenoate
Reaktionsgleichung
[CH2:1]([CH:9]([C:15](OCC)=O)[C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].IC[CH2:22][CH2:23][C:24]([F:30])([F:29])[C:25]([F:28])([F:27])[F:26]>>[F:29][C:24]([F:30])([C:25]([F:28])([F:27])[F:26])[CH2:23][CH2:22][CH2:15][CH:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8])[C:10]([O:12][CH2:13][CH3:14])=[O:11]Komponenten
3
Versuchsvorschrift
Starting with the diethyl 2-(7-octenyl)malonate prepared in Example 5 and the 1-iodo-4,4,5,5,5-pentafluoropentane prepared in Example 1, the same procedure as shown in Example 5 was repeated to give ethyl 2-(4,4,5,5,5-pentafluoropentyl)-9-decenoate.
Quellen und Nachweise
- ORD-Eintrag
- ord-012ea590a1ce4467b5b8f69b6f7efe10
- Quelldatensatz
- uspto-grants-2003_04
- Patentnummer
- US06552068B1
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