HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3-Dimethylaniline → HCID 20481270, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3-Dimethylaniline | HCID 6893 | — |
| Edukt | 2-(chloromethyl)-4,5-dihydro-1H-imidazole hydrochloride | HCID 2760928 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 20481270 | HCID 20481270 | 77% |
Reaktionsschritte
31 g of 2-chloromethyl-2-imidazoline hydrochloride and 48.4 g of 2,3-dimethylaniline are refluxed for 5 hours in 65 ml of absolute ethanol. After cooling, the crystallised substance is collected by suction and recrystallised from water, affording 36 g (77% yield) of the final product with a melting point of 242° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04254133 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-e06acf45d0b04201b442b52954b92b8f |
| Quellennotiz | uspto-grants-1981_03 |