HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetylene → 1-Chloro-1-octen-3-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetylene | HCID 6326 | — |
| Edukt | Hexanoyl chloride | HCID 67340 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Produkt | 1-Chloro-1-octen-3-one | HCID 54514915 | 94% |
Reaktionsschritte
This compound is prepared according to the procedure of Price and Pappalardo [C. C. Price and J. A. Pappalardo, Org. Syn, 32, 27 (1952)] from hexanoyl chloride, acetylene, and aluminum chloride in 94% yield, bp 51°-52° C. (0.1 mm); λ max 1680, 1595, 941 cm-1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04254285 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-c71981136930439f9fc57a6a9cfed018 |
| Quellennotiz | uspto-grants-1981_03 |