HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aniline → Methanimidic acid, N-phenyl-, ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aniline | HCID 6115 | — |
| Edukt | Ethyl orthoformate | HCID 31214 | — |
| Edukt | N,N'-Diphenylformamidine | HCID 94888 | — |
| Produkt | Methanimidic acid, N-phenyl-, ethyl ester | HCID 111236 | — |
Reaktionsschritte
The synthesis is achieved in three steps. The first step is the preparation of N,N′-diphenyl formamidine (by the reaction of aniline with triethyl orthoformate). This intermediate is then further reacted with triethyl orthoformate to produce ethyl N-phenylimidoformate. The final step is the reaction of ethyl phenylimidoformate with 4-aminostyrene to give the product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07208557B2 |
| Quelldatensatz | uspto-grants-2007_04 |
| ORD ID | ord-1ef5853adf0c4154b000c2a12196db5b |
| Quellennotiz | uspto-grants-2007_04 |