Chloride → 2-Methyl-3,4,6-trifluorobenzoyl chloride

HRID 1273

Reaktionsgleichung

Reaktionsgleichung von HRID 1273
[CH3:1][C:2]1[C:10]([F:11])=[C:9]([F:12])[CH:8]=[C:7]([F:13])[C:3]=1[C:4](O)=[O:5].[Cl-:14]>>[CH3:1][C:2]1[C:10]([F:11])=[C:9]([F:12])[CH:8]=[C:7]([F:13])[C:3]=1[C:4]([Cl:14])=[O:5]

Komponenten

3

Edukt 2

HCID 312ChlorideHCID 101303052-Methyl-3,4,6-trifluorobenzoic acid

Produkt 1

HCID 150076072-Methyl-3,4,6-trifluorobenzoyl chloride

Versuchsvorschrift

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

Aufarbeitung

  1. temperaturethe mixture is refluxed for 1 hour
  2. concentrationAfter concentrating

Quellen und Nachweise

ORD-Eintrag
ord-141b4f862c4146f6950ca566cd749152
Quelldatensatz
uspto-grants-1998_03
Patentnummer
US05723648

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