HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
DL-Phenylalanine, methyl ester → (R)-Methyl 2-amino-3-phenylpropanoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | DL-Phenylalanine, methyl ester | HCID 75737 | — |
| Edukt | N-(Benzyloxycarbonyl)-L-aspartyl-L-phenylalanine methyl ester | HCID 10159630 | — |
| Produkt | (R)-Methyl 2-amino-3-phenylpropanoate | HCID 853474 | 62,3% |
Reaktionsschritte
Example 17 was repeated except for using DL-phenylalanine methyl ester instead of L-phenylalanine methyl ester to obtain 756 mg of an addition compound of N-benzyloxycarbonyl-L-aspartyl L-phenylalanine methyl ester and D-phenyl alanine methyl ester (1:1) (melting point: 105° to 111° C.; yield: 62.3% based on N-benzyloxycarbonyl L-aspartic acid).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04256836 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-ce242cf6324f4ad7b110d3fb48e26462 |
| Quellennotiz | uspto-grants-1981_03 |