HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 3,7-Dihydroxyflavylium chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 2,4-Dihydroxybenzaldehyde | HCID 7213 | — |
| Edukt | Ethanone, 2-(acetyloxy)-1-phenyl- | HCID 222851 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | 3,7-Dihydroxyflavylium chloride | HCID 20481738 | — |
Reaktionsschritte
79 g of 2,4-dihydroxybenzaldehyde were dissolved at room temperature in 800 ml of anhydrous ethyl acetate and 106 g of omega-acetoxyacetophenone were added to the solution. The reaction mixture was brought to 0° C. under agitation and gaseous hydrochloric acid added to saturation. After standing for 24 hours at room temperature, crystallisation of the product began and it was filtered and dried at 40° C. in the presence of NaOH. There were obtained 95 g of 3,7-dihydroxyflavilium chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04258055 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-5061ef8a3f24490ea5f4b54912055992 |
| Quellennotiz | uspto-grants-1981_03 |