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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 127946Erstellt: 24. Oktober 2026

Hydrochloric Acid → 3,7-Dihydroxyflavylium chloride

https://huagongshe.com/de/reaction/127946

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
Edukt2,4-DihydroxybenzaldehydeHCID 7213—
EduktEthanone, 2-(acetyloxy)-1-phenyl-HCID 222851—
LösungsmittelEthyl AcetateHCID 8857—
Produkt3,7-Dihydroxyflavylium chlorideHCID 20481738—

Reaktionsschritte

79 g of 2,4-dihydroxybenzaldehyde were dissolved at room temperature in 800 ml of anhydrous ethyl acetate and 106 g of omega-acetoxyacetophenone were added to the solution. The reaction mixture was brought to 0° C. under agitation and gaseous hydrochloric acid added to saturation. After standing for 24 hours at room temperature, crystallisation of the product began and it was filtered and dried at 40° C. in the presence of NaOH. There were obtained 95 g of 3,7-dihydroxyflavilium chloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04258055
Quelldatensatzuspto-grants-1981_03
ORD IDord-5061ef8a3f24490ea5f4b54912055992
Quellennotizuspto-grants-1981_03