HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dioctadecylamine → HCID 20433003, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dioctadecylamine | HCID 66989 | — |
| Edukt | Ethyl 4-bromobutyrate | HCID 76300 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | HCID 20433003 | HCID 20433003 | 58,2% |
Reaktionsschritte
A solution of dioctadecylamine (5.2 g., 0.01 mole), ethyl 4-bromobutyrate (1.95 g., 0.01 mole) and toluene (50 ml.) is heated at reflux for sixteen hours, then cooled and concentrated in vacuo to a semi-solid oil. The oil is triturated with ethylacetate, filtered, and the filtrate washed with water, then dried (Na2SO4). Removal of the solvent gives the product as an oil (3.7 g.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04258061 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-24c64bf11f244c4e8505596e5ea82237 |
| Quellennotiz | uspto-grants-1981_03 |