(Phenylmethoxy)acetaldehyde → (RS)-4-[1-(2-Benzyloxy-ethyl)-pyrrolidine-3-sulfonyl]-phenol
Reaktionsgleichung
FC(F)(F)C(O)=O.[NH:8]1[CH2:12][CH2:11][CH:10]([S:13]([C:16]2[CH:21]=[CH:20][C:19]([OH:22])=[CH:18][CH:17]=2)(=[O:15])=[O:14])[CH2:9]1.[CH2:23]([O:30][CH2:31][CH:32]=O)[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[CH2:23]([O:30][CH2:31][CH2:32][N:8]1[CH2:12][CH2:11][CH:10]([S:13]([C:16]2[CH:21]=[CH:20][C:19]([OH:22])=[CH:18][CH:17]=2)(=[O:15])=[O:14])[CH2:9]1)[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1Komponenten
3
Versuchsvorschrift
The title compound, MS: m/e=362.2 (M+H+) was prepared from (RS)-4-(pyrrolidine-3-sulfonyl)-phenol trifluoroacetic acid salt and benzyloxyacetaldehyde.
Quellen und Nachweise
- ORD-Eintrag
- ord-a2028686e1464945957b6a45afeea816
- Quelldatensatz
- uspto-grants-2002_09