Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1280819Erstellt: 26. Oktober 2026

N-(2-phenyl-phenylmethyl)-phthalimide → 1-Biphenyl-2-ylmethanamine

https://huagongshe.com/reaction/1280819

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN-(2-phenyl-phenylmethyl)-phthalimideHCID 18426122—
LösungsmittelHydrazine hydrate (1:1)HCID 24654—
Produkt1-Biphenyl-2-ylmethanamineHCID 26336678,9%

Reaktionsschritte

N-(2-Phenyl-phenylmethyl)-phthalimide (6.5 g) in 25 cc of hydrazine hydrate were stirred at room temperature overnight. Ice water was added and the solid separated by filtration. The filtrate was salted out with brine and extracted with ethyl acetate. The ethyl acetate extract was washed with water, dried over magnesium sulfate, filtered and concentrated to dryness to afford 3 g of subtitled product as an oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06451839B1
Quelldatensatzuspto-grants-2002_09
ORD IDord-92513ac2ba0f4915b383c24c79517d71
Quellennotizuspto-grants-2002_09