HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 18422335, Verbindung → Ethyl 2-(2-amino-4,5-difluoroanilino)benzo[b]thiophene-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 18422335 | HCID 18422335 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | HCID 178418390 | HCID 178418390 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Ethyl 2-(2-amino-4,5-difluoroanilino)benzo[b]thiophene-3-carboxylate | HCID 18422150 | — |
Reaktionsschritte
In the same manner as in Starting Material Synthesis Example 19 and using ethyl 2-(4,5-difluoro-2-nitroanilino)benzo[b]thiophene-3-carboxylate, ethyl acetate, 10% palladium-carbon and hydrogen (60 atm kg/cm2), ethyl 2-(2-amino-4,5-difluoroanilino)benzo[b]thiophene-3-carboxylate is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06455521B1 |
| Quelldatensatz | uspto-grants-2002_09 |
| ORD ID | ord-47b36bfa83ca42a5b3a0d0fee59e2925 |
| Quellennotiz | uspto-grants-2002_09 |