HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → HCID 178527203, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Oxalic Acid | HCID 971 | — |
| Edukt | Oxo(oxostibanyloxy)stibane | HCID 27652 | — |
| Edukt | Ammonium metavanadate | HCID 516859 | — |
| Edukt | (Ethanedioato(2-)-kappaO1,kappaO2)oxovanadium | HCID 21900408 | — |
| Produkt | HCID 178527203 | HCID 178527203 | — |
Reaktionsschritte
27.58 grams of Sb2O3 were added to a vanadyl oxalate solution prepared by adding 24 grams of oxalic acid (H2C2O4.2H2O) to a warm (~55° C.) aqueous mixture of 11.06 grams of ammonium metavanadate (NH4VO3) in 25 ml of water. The reaction mixture was dried at 110° C. and the vanadium antimonate precursor so obtained was calcined in an air flow at 550° C. for 2 hours.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04565658 |
| Quelldatensatz | uspto-grants-1986_01 |
| ORD ID | ord-defdcf082896443da8a3d67afe5eae75 |
| Quellennotiz | uspto-grants-1986_01 |