HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol, 2-fluoro-2,2-dinitro- → 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol, 2-fluoro-2,2-dinitro- | HCID 28189 | — |
| Edukt | Acetic acid, trifluoro-, (methylnitroamino)methyl ester | HCID 13352131 | — |
| Produkt | 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane | HCID 13352133 | — |
Reaktionsschritte
reacting one mole of 2-nitro-2-azapropyl trifluoroacetate with one mole of 2-fluoro-2,2-dinitroethanol in a polar solvent at a temperature of from 0° C. to 40° C. to form 1-fluoro-1,1,5-trinitro-3-oxa-5azahexane, wherein the reaction is run under vacuum to remove trifluoroacetic acid generated by the reaction; and
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04567296 |
| Quelldatensatz | uspto-grants-1986_01 |
| ORD ID | ord-45804309d9454f8fb4d6d054f98606be |
| Quellennotiz | uspto-grants-1986_01 |