HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromopropane → 2-Methyl-3-propoxypyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromopropane | HCID 7840 | — |
| Edukt | 2-Methylpyridin-3-ol | HCID 70719 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Lösungsmittel | 1-Propanol | HCID 1031 | — |
| Produkt | 2-Methyl-3-propoxypyridine | HCID 19374328 | — |
Reaktionsschritte
3-Hydroxy-2-methylpyridine (50 g) was added to a solution of sodium (11.6 g) in propan-1-ol (250 ml) and the mixture treated with 1-bromopropane (51 ml) in propan-1-ol (50 ml) to give 2-methyl-3-propoxypyridine, b.p. 96°-104° C. (30 mmHg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05464781 |
| Quelldatensatz | uspto-grants-1995_11 |
| ORD ID | ord-9e6b084079f44c2d845926ea4abf4213 |
| Quellennotiz | uspto-grants-1995_11 |