2-Mercaptoethanol → 3-{[2-(2-Cyanoethoxy)ethyl]sulfanyl}propanenitrile
Reaktionsgleichung
[SH:1][CH2:2][CH2:3][OH:4].[C:5](#[N:8])[CH:6]=[CH2:7].[OH-].[CH2:10]([N+:17](C)(C)C)[C:11]1C=CC=C[CH:12]=1>>[C:10](#[N:17])[CH2:11][CH2:12][O:4][CH2:3][CH2:2][S:1][CH2:7][CH2:6][C:5]#[N:8]Komponenten
4
Versuchsvorschrift
4-Oxa-7-thiadecanedinitrile was prepared according to the procedure of Example 1 using 2-mercaptoethanol (25.0 g; 0.32 moles), acrylonitrile (34.0 g; 0.64 moles) and benzyltrimethylammonium hydroxide (40% in methanol; 1 ml) as the catalyst.
Quellen und Nachweise
- ORD-Eintrag
- ord-a8b355b3865f4037948200fd35e91e53
- Quelldatensatz
- uspto-grants-1976_10
- Patentnummer
- US03984336
Notizen zur Reaktion
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